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Setup List
Holder Status Name ExpNo Experiment User Time Title
1 Completed 200925-mdn 2 N 1H 1H experiment mdn 00:01:07 Supervisor Stenzel DMA-Ribo-1/2-60min
2 Completed 200925-mdn 3 N 1H 1H experiment mdn 00:01:07 Supervisor Stenzel DMA-Ribo-2/2-30min
3 Completed 200925-mdn 4 N 1H 1H experiment mdn 00:01:07 Supervisor Stenzel DMA-Ribo-2/2-60min
4 Completed 200925-ehw 1 N 1H 1H experiment ehw 00:02:15 Supervisor Boyer rnzf post synthesis
5 Completed 200925-ehw 2 N 1H 1H experiment ehw 00:02:15 Supervisor Boyer paaptac-fluorescein
6 Completed 200925-fis 3 N 1H 1H experiment fis 00:01:07 Supervisor Zetterlund DT4 1h
7 Completed 200925-fis 4 N 1H 1H experiment fis 00:01:07 Supervisor Zetterlund DT4 2h
8 Completed 200925-fis 5 N 1H 1H experiment fis 00:01:07 Supervisor Zetterlund DT4 3h
9 Completed 200925-fis 6 N 1H 1H experiment fis 00:01:07 Supervisor Zetterlund DT4 4h
10 Completed 200925-fis 7 N 1H 1H experiment fis 00:01:07 Supervisor Zetterlund DT4 5h
11 Completed 200925-fis 8 N 1H 1H experiment fis 00:01:07 Supervisor Zetterlund DT4 5.5h
21 Completed 200925-mdt 1 N 1H 1H experiment mdt 00:01:07 Supervisor Harper [bmim]Cl in d6-acetone Use this NMR for experimental
22 Completed 200925-mdt 2 N 1H 1H experiment mdt 00:01:07 Supervisor Harper [(mim)2m][NTf2]2 in DMSO Use this NMR for experimental
23 Completed 200925-ydx 1 N 1H 1H experiment ydx 00:04:30 Supervisor Stenzel SC18pMAA-b-HPMA F=10 1:1 D/M 5h
24 Completed 200925-ydx 2 N 1H 1H experiment ydx 00:04:30 Supervisor Stenzel SC18pMAA-b-HPMA26 DMAC 5h F=24
47 Completed 200925-ysu 1 N 1H 1H experiment ysu 00:01:07 Supervisor Hunter ysu2004 crude 2
54 Completed 200925-shs 1 N 1H 1H experiment shs 00:02:15 Supervisor Kumar shs-4-47 in CDCl3
55 Completed 200925-cas 1 N 1H 1H experiment cas 00:01:07 Supervisor Thordarson 200925 DMSO CS-1-1 FSRPAFL
55 Completed 200925-cas 4 N 13C.night 13C experiment; use td0 to add scans cas 01:13:50 Supervisor Thordarson 200925 DMSO CS-1-1 FSRPAFL
55 Completed 200925-cas 5 N 13C.dept135 DEPT 135 experiment; 128 scans cas 00:10:46 Supervisor Thordarson 200925 DMSO CS-1-1 FSRPAFL
56 Completed 200925-cas 6 N 1H 1H experiment cas 00:01:07 Supervisor Thordarson 200925 DMSO CS-1-31 (T7)
56 Completed 200925-cas 7 N 13C.night 13C experiment; use td0 to add scans cas 01:13:50 Supervisor Thordarson 200925 DMSO CS-1-31 (T7)
56 Completed 200925-cas 8 N 13C.dept135 DEPT 135 experiment; 128 scans cas 00:10:46 Supervisor Thordarson 200925 DMSO CS-1-31 (T7)
57 Completed 200925-jsk 1 N 1H 1H experiment jsk 00:01:07 Supervisor Wich JK174 extra purification
58 Completed 200925-jsk 2 N 1H 1H experiment jsk 00:01:07 Supervisor Wich JK184 extra purification
59 Completed 200925-jsk 3 N 1H 1H experiment jsk 00:01:07 Supervisor Wich JK190 extra purification
60 Completed 200925-mdn 1 N 1H 1H experiment mdn 00:01:07 Supervisor Stenzel DMA-Ribo-1/2-30min
History List
Holder Time Name ExpNo Experiment User Load Atma Spin Lock Shim Acq Proc Title Remarks
11 21:26:32 200925-fis 8 1H fis + + + + + + - Supervisor Zetterlund DT4 5.5h
10 21:19:27 200925-fis 7 1H fis + + + + + + + Supervisor Zetterlund DT4 5h
9 21:12:42 200925-fis 6 1H fis + + + + + + + Supervisor Zetterlund DT4 4h
8 21:05:43 200925-fis 5 1H fis + + + + + + + Supervisor Zetterlund DT4 3h
7 20:58:42 200925-fis 4 1H fis + + + + + + + Supervisor Zetterlund DT4 2h
6 20:51:43 200925-fis 3 1H fis + + + + + + + Supervisor Zetterlund DT4 1h
5 20:43:31 200925-ehw 2 1H ehw + + + + + + + Supervisor Boyer paaptac-fluorescein
4 20:35:01 200925-ehw 1 1H ehw + + + + + + + Supervisor Boyer rnzf post synthesis
3 20:28:28 200925-mdn 4 1H mdn + + + + + + + Supervisor Stenzel DMA-Ribo-2/2-60min
2 20:21:48 200925-mdn 3 1H mdn + + + + + + + Supervisor Stenzel DMA-Ribo-2/2-30min
1 20:15:15 200925-mdn 2 1H mdn + + + + + + + Supervisor Stenzel DMA-Ribo-1/2-60min
60 20:08:25 200925-mdn 1 1H mdn + + + + + + + Supervisor Stenzel DMA-Ribo-1/2-30min
59 20:01:06 200925-jsk 3 1H jsk + + + + + + + Supervisor Wich JK190 extra purification
58 19:53:24 200925-jsk 2 1H jsk + + + + + + + Supervisor Wich JK184 extra purification
57 19:45:19 200925-jsk 1 1H jsk + + + + + + + Supervisor Wich JK174 extra purification
56 19:32:45 200925-cas 8 13C.dept135 cas - + + - - + + Supervisor Thordarson 200925 DMSO CS-1-31 (T7)
56 18:17:11 200925-cas 7 13C.night cas - + + - - + + Supervisor Thordarson 200925 DMSO CS-1-31 (T7)
56 18:10:08 200925-cas 6 1H cas + + + + + + + Supervisor Thordarson 200925 DMSO CS-1-31 (T7)
55 17:57:36 200925-cas 5 13C.dept135 cas - + + - - + + Supervisor Thordarson 200925 DMSO CS-1-1 FSRPAFL
55 16:41:43 200925-cas 4 13C.night cas - + + - - + + Supervisor Thordarson 200925 DMSO CS-1-1 FSRPAFL
55 16:34:13 200925-cas 1 1H cas + + + + + + + Supervisor Thordarson 200925 DMSO CS-1-1 FSRPAFL
54 16:17:59 200925-shs 1 1H shs + + + + + + + Supervisor Kumar shs-4-47 in CDCl3
47 15:35:48 200925-ysu 1 1H ysu + + + + + + + Supervisor Hunter ysu2004 crude 2
24 15:22:38 200925-ydx 2 1H ydx + + + + + + + Supervisor Stenzel SC18pMAA-b-HPMA26 DMAC 5h F=24
23 15:12:13 200925-ydx 1 1H ydx + + + + + + + Supervisor Stenzel SC18pMAA-b-HPMA F=10 1:1 D/M 5h
22 13:59:29 200925-mdt 2 1H mdt + + + + + + + Supervisor Harper [(mim)2m][NTf2]2 in DMSO Use this NMR for experimental
21 13:49:08 200925-mdt 1 1H mdt + + + + + + + Supervisor Harper [bmim]Cl in d6-acetone Use this NMR for experimental
53 12:28:02 200925-cas 2 19F cas - + + - - + + Supervisor Thordarson 200925 CDCl3 CS-1-41 dialysed
53 12:20:05 200925-cas 1 1H cas + + + + + + + Supervisor Thordarson 200925 CDCl3 CS-1-41 dialysed
52 12:11:51 200925-dbr 2 1H dbr + + + + + + + Supervisor Peeks DB-1-044 Recryst white crystals old CDCl3
51 12:04:43 200925-gec 2 1H gec + + + + + + + Supervisor Hunter GC-4-060_02aliquot_D2O_300
50 11:58:03 200925-gec 1 1H gec + + + + + + + Supervisor Hunter GC-2-042_insolEtOAc-2020check_DMSO_300
49 11:51:26 200925-moa 2 1H moa + + + + + + + Supervisor Hunter MOA 1.108 (ethyl acetate filterate) in dmso
48 11:44:43 200925-moa 1 1H moa + + + + + + + Supervisor Hunter MOA 1.108 (ethyl acetate ppt) in dmso
46 11:34:40 200925-tjh 2 1H tjh + + + + + + + Supervisor Morris THv23 Crude MeOD 300MHz (Gyro) 25/9/20
45 11:26:03 200925-tjh 1 1H tjh + + + + + + + Supervisor Morris tjh OG01 Crude CDCl3 300MHz (Gyro) 25/9/20
44 11:18:01 200925-fis 2 1H fis + + + + + + + Supervisor Zetterlund fis244
43 11:09:36 200925-fis 1 1H fis + + + + + + + Supervisor Zetterlund fis243 E
42 11:01:25 200925-dbr 1 1H dbr + + + + + + + Supervisor Peeks DB-1-044 colourless crystals orange soln
41 10:50:46 200925-prj 4 1H prj + + + + + + + Supervisor Boyer AAPTAC:PEAm 100DPn T1
40 10:40:26 200925-prj 3 1H prj + + + + + + + Supervisor Boyer AAPTAC:PEAm 40DPn T1
39 10:29:59 200925-prj 2 1H prj + + + + + + + Supervisor Boyer AAPTAC:PEAm 100DPn T0
38 10:19:08 200925-prj 1 1H prj + + + + + + + Supervisor Boyer AAPTAC:PEAm 40DPn T0
37 10:08:14 200925-dne 1 1H dne + + + + + + + Supervisor Morris DANE41 WU in CDCl3
36 10:01:28 200924-mdh 1 1H mdh + + + + + + + Supervisor G. Mao Succinylated TPGS in D2O
35 08:21:21 200924-moa 29 13C.day moa - + + - - + + Supervisor Hunter MOA. 1.104( acetone wash filtrate, 2nd recrystal) in dmso. no need to wash it with acetone as its pure enough.
35 08:08:15 200924-moa 28 1H13C.hmbc moa - + + - - + + Supervisor Hunter MOA. 1.104( acetone wash filtrate, 2nd recrystal) in dmso. no need to wash it with acetone as its pure enough.
35 07:49:33 200924-moa 27 1H13C.hsqc.aded moa - + + - - + x Supervisor Hunter MOA. 1.104( acetone wash filtrate, 2nd recrystal) in dmso. no need to wash it with acetone as its pure enough.
35 07:38:22 200924-moa 26 1H.cosy moa - + + - - + + Supervisor Hunter MOA. 1.104( acetone wash filtrate, 2nd recrystal) in dmso. no need to wash it with acetone as its pure enough.
35 07:23:41 200924-moa 25 1H moa + + + + + + + Supervisor Hunter MOA. 1.104( acetone wash filtrate, 2nd recrystal) in dmso. no need to wash it with acetone as its pure enough.
34 05:43:35 200924-moa 24 13C.day moa - + + - - + + Supervisor Hunter MOA. 1.104(dmf recrystal) in dmso. no need to wash it with acetone as its pure enough.
34 05:30:26 200924-moa 23 1H13C.hmbc moa - + + - - + + Supervisor Hunter MOA. 1.104(dmf recrystal) in dmso. no need to wash it with acetone as its pure enough.
34 05:11:44 200924-moa 22 1H13C.hsqc.aded moa - + + - - + + Supervisor Hunter MOA. 1.104(dmf recrystal) in dmso. no need to wash it with acetone as its pure enough.
34 05:00:33 200924-moa 21 1H.cosy moa - + + - - + + Supervisor Hunter MOA. 1.104(dmf recrystal) in dmso. no need to wash it with acetone as its pure enough.
34 04:48:18 200924-moa 20 1H moa + + + + + + + Supervisor Hunter MOA. 1.104(dmf recrystal) in dmso. no need to wash it with acetone as its pure enough.
33 03:08:10 200924-moa 19 13C.day moa - + + - - + + Supervisor Hunter MOA. 1.108 (ethyl acetate filtrate) in dmso. mass was 375 and 376 in 3:1 ratio
33 02:55:03 200924-moa 18 1H13C.hmbc moa - + + - - + + Supervisor Hunter MOA. 1.108 (ethyl acetate filtrate) in dmso. mass was 375 and 376 in 3:1 ratio
33 02:36:21 200924-moa 17 1H13C.hsqc.aded moa - + + - - + + Supervisor Hunter MOA. 1.108 (ethyl acetate filtrate) in dmso. mass was 375 and 376 in 3:1 ratio
33 02:25:08 200924-moa 16 1H.cosy moa - + + - - + + Supervisor Hunter MOA. 1.108 (ethyl acetate filtrate) in dmso. mass was 375 and 376 in 3:1 ratio
33 02:12:41 200924-moa 15 1H moa + + + + + + + Supervisor Hunter MOA. 1.108 (ethyl acetate filtrate) in dmso. mass was 375 and 376 in 3:1 ratio
32 00:32:33 200924-moa 14 13C.day moa - + + - - + + Supervisor Hunter MOA. 1.108 (ethyl acetate ppt) recrystal in dmso. mass was 379.17 and 381.17 in 3:1 ratio
32 00:19:23 200924-moa 13 1H13C.hmbc moa - + + - - + + Supervisor Hunter MOA. 1.108 (ethyl acetate ppt) recrystal in dmso. mass was 379.17 and 381.17 in 3:1 ratio
32 00:00:37 200924-moa 12 1H13C.hsqc.aded moa - + + - - + + Supervisor Hunter MOA. 1.108 (ethyl acetate ppt) recrystal in dmso. mass was 379.17 and 381.17 in 3:1 ratio
32 23:49:26 200924-moa 11 1H.cosy moa - + + - - + + Supervisor Hunter MOA. 1.108 (ethyl acetate ppt) recrystal in dmso. mass was 379.17 and 381.17 in 3:1 ratio
32 23:36:50 200924-moa 10 1H moa + + + + + + + Supervisor Hunter MOA. 1.108 (ethyl acetate ppt) recrystal in dmso. mass was 379.17 and 381.17 in 3:1 ratio
31 23:29:59 200924-lxu 2 1H lxu + + + + + + + Supervisor Neville coumarin_2_DMSO
30 23:22:52 200924-dbr 3 1H dbr + + + + + + + Supervisor Peeks BKH-1-001 Frac 2
29 23:15:55 200924-dbr 4 1H dbr + + + + + + + Supervisor Peeks BKH-1-001 Frac 1
28 23:08:15 200924-dbr 1 1H dbr + + + + + + + Supervisor Peeks DB-1-045 White precipitate
27 23:00:43 200924-pir 1 1H pir + + + + + + + Supervisor Hunter PR4.34 Cr
26 20:58:52 200924-vra 3 13C.night vra + + + + + + + Supervisor Kumar VRA-9-28 lauramido betaine in cdcl3
25 19:01:47 200924-vra 2 13C.night vra - + + - - + + Supervisor Kumar VRA-9-30 dienamido betaine
25 18:53:10 200924-vra 1 1H vra + + + + + + + Supervisor Kumar VRA-9-30 dienamido betaine
24 18:43:14 200924-moa 9 1H moa + + + + + + + Supervisor Hunter MOA 1.104 (2nd recrystal or acetone filtrate) in dmso dmf recrystal was washed with cold acetone this is supposed to be the pure acridine nitro ester M+H was 361.17
23 18:33:18 200924-moa 8 1H moa + + + + + + + Supervisor Hunter MOA 1.104 (dmf recrystal) in dmso starting maetrial for 1.108 reaction. not pure enough, thats why the yild was low in the 1.108 reaction
22 18:23:16 200924-moa 7 1H moa + + + + + + + Supervisor Hunter MOA 1.108(ethyl acetate filtrate) in DMSO org fraction was washed with hot ethyl acetate and filter it to get the precipitate. mass spectrum confirms it is the non chlorinated ester M+H 375, 376 in 1:3ratio
21 18:12:59 200924-moa 6 1H moa + + + + + + + Supervisor Hunter MOA 1.108(ethyl acetate precipitate) in DMSO org fraction was washed with hot ethyl acetate and filter it to get rid of the precipitate. mass spectrum confirms it is the chlorinated ester M+H 379, 381(for chlorine isotope) in 1:3ratio yiled was only 10%
20 18:02:20 200924-ydx 1 1H ydx + + + + + + + Supervisor Stenzel SC18pMAA-b-HPMA | DMAc | 5h
19 17:53:39 200924-lzg 5 1H lzg + + + + + + + Supervisor Stenzel pegmema-4
18 17:45:27 200924-lzg 4 1H lzg + + + + + + + Supervisor Stenzel pegmema-3
17 17:37:19 200924-lzg 3 1H lzg + + + + + + + Supervisor Stenzel pegmema-2
16 17:29:12 200924-lzg 2 1H lzg + + + + + + + Supervisor Stenzel pegmema-1
15 17:21:07 200924-lzg 1 1H lzg + + + + + + + Supervisor Stenzel T=0
14 17:14:28 200924-leh 2 1H leh + + + + + + + Supervisor Neville 3Nap Frac 3 check DMSO
13 17:00:22 200924-leh 3 13C.day leh - + + - - + + Supervisor Neville 3Nap-frac 2 check DMSO
13 16:53:03 200924-leh 1 1H leh + + + + + + + Supervisor Neville 3Nap-frac 2 check DMSO
12 16:20:06 200924-vkk 1 1H vkk + x + + + + + Supervisor Wich VKK-2309 AcAmy (10min) ATM Failed
9 15:53:50 200924-shs 1 1H shs + + + + + + + Supervisor Kumar shs-4-54
8 14:24:40 200924-tlm 1 1H tlm + + + + + + + Supervisor Morris TMD.09 - check. CDCl3.
7 14:17:22 200924-ysu 1 1H ysu + + + + + + + Supervisor Hunter crude product ys2004
6 14:10:18 200924-mdt 1 1H mdt + + + + + + + Supervisor Harper C1 biscation after ether washes and high vac DMSO
5 13:19:21 200924-moa 5 13C.day moa - + + - - + + Supervisor Hunter MOA 1.108 (organic FRcation ) dried in DMSO
5 13:06:16 200924-moa 4 1H13C.hmbc moa - + + - - + + Supervisor Hunter MOA 1.108 (organic FRcation ) dried in DMSO
5 12:47:16 200924-moa 3 1H13C.hsqc.aded moa - + + - - + + Supervisor Hunter MOA 1.108 (organic FRcation ) dried in DMSO
5 12:36:05 200924-moa 2 1H.cosy moa - + + - - + + Supervisor Hunter MOA 1.108 (organic FRcation ) dried in DMSO
5 12:29:29 200924-moa 1 1H moa + + + + + + + Supervisor Hunter MOA 1.108 (organic FRcation ) dried in DMSO
4 11:55:41 200924-ksd 1 1H ksd + + + + + + + Supervisor Hunter KSD-1-15a (recrst)
3 11:45:53 200924-lxu 1 1H lxu + + + + + + + Supervisor Neville coumarin_2_cdod
2 11:40:55 200924-cas 2 19F cas - + + - - + + Supervisor Thordarson 200924 CDCl3 CS-1-41 crude
2 11:33:22 200924-cas 1 1H cas + + + + + + + Supervisor Thordarson 200924 CDCl3 CS-1-41 crude
1 10:22:47 200924-tmk 1 1H tmk + + + + + + + Supervisor Morris tmk-tmkb5-p-nahco3-cdcl3