Icon NMR logo

IconNMR Automation Run Status:
Day Experiments: 10:52
Busy Until: Wed 06:57
Night Experiments: 00:00

Setup List
Holder Status Name ExpNo Experiment User Time Title
1 Submitted 200407-jpj 3 N 1H 1H experiment jpj 00:01:00 Supervisor Kumar distilled formic acid
2 Submitted 200407-yim 2 N 1H 1H experiment yim 00:01:00 Supervisor Stenzel z-lysine monomer ( 3 recrysta)
3 Submitted 200407-tat 3 N 1H 1H experiment tat 00:05:03 Supervisor Nguyen CDCl3_P2-A42_F4-10
4 Submitted 200407-tat 4 N 1H 1H experiment tat 00:05:03 Supervisor Nguyen CDCl3_P2-A42_F12-22
5 Submitted 200407-tat 5 N 1H 1H experiment tat 00:05:03 Supervisor Nguyen CDCl3_P2-A42_F23-43
6 Error 200407-dme 1 N 1H 1H experiment dme 00:01:00 Supervisor Stenzel Acid 3 crude 7/04/2020
7 Error 200405-jwd 6 N 1H.noesy jwd 00:33:03 Supervisor Morris jwd-H103; Nphenyl pyrazole; DMSO; NOESY; 400MHz
8 Submitted 200407-tat 6 N 1H 1H experiment tat 00:14:56 Supervisor Nguyen CDCl3_P2-A41-2_PTLC_F1_1H
8 Submitted 200407-tat 7 N 13C.night 13C experiment; use td0 to add scans tat 02:04:18 Supervisor Nguyen CDCl3_P2-A41-2_PTLC_F1_13C
9 Submitted 200407-tjh 1 N 1H 1H experiment tjh 00:01:00 Supervisor Morris THiii43 Crude CDCl3 400MHz (Gauss) 7/4/20
29 Completed 200407-mjh 5 N 1H 1H experiment mjh 00:01:00 Supervisor Chapman MH1.14E pA-MA. 0% HEMA. DP800. 1/800 Cye3.
30 Completed 200407-mjh 6 N 1H 1H experiment mjh 00:01:00 Supervisor Chapman MH1.14F pA-MA/HEMA. 10% HEMA. DP800. 1/800 Cye3.
31 Completed 200407-mjh 7 N 1H 1H experiment mjh 00:01:00 Supervisor Chapman MH1.14G pA-MA/HEMA. 20% HEMA. DP800. 1/800 Cye3.
32 Completed 200407-mjh 8 N 1H 1H experiment mjh 00:01:00 Supervisor Chapman MH1.14H pA-MA/HEMA. 50% HEMA. DP800. 1/800 Cye3.
33 Completed 200407-jwd 4 N 1H 1H experiment jwd 00:01:00 Supervisor Morris jwd; H103-pyraozle; DMF; 400MHz
34 Completed 200407-mjh 9 N 1H 1H experiment mjh 00:01:00 Supervisor Chapman MH1.14I pA-MA. DP400. 10x cye3.
35 Completed 200407-moa 1 N 1H 1H experiment moa 00:01:00 Supervisor Hunter MOA1.066 CRude (may have Toluene) in CDCl3
36 Completed 200407-ydx 1 N 1H 1H experiment ydx 00:01:00 Supervisor Stenzel Caro - CH22 free radical polymerisation
37 Completed 200407-ydx 2 N 1H 1H experiment ydx 00:04:03 Supervisor Stenzel PFP-1
38 Completed 200407-ydx 3 N 1H 1H experiment ydx 00:04:03 Supervisor Stenzel PFP-2
39 Completed 200407-ydx 4 N 1H 1H experiment ydx 00:04:03 Supervisor Stenzel DP-C18
40 Completed 200407-pir 2 N 1H 1H experiment pir 00:01:00 Supervisor Hunter PR3.32 THF-check
41 Completed 200407-jwd 5 N 1H 1H experiment jwd 00:01:00 Supervisor Morris jwd; H103-pyrazole; dmf; 400MHz 2
41 Completed 200407-jwd 6 N 1H13C.hsqc.aded jwd 00:10:52 Supervisor Morris jwd; H103-pyrazole; dmf; 400MHz; HSQC
42 Completed 200407-rra 1 N 1H 1H experiment rra 00:02:01 Supervisor Stenzel RR34_PHEA-Semicarbazide
43 Completed 200407-hgf 1 N 1H 1H experiment hgf 00:01:00 Supervisor Martina HF1.6 re.cryst.NIPAM CDCl3
44 Completed 200407-jwd 7 N 1H 1H experiment jwd 00:01:00 Supervisor Morris jwd-H109-NH2-pyrazole; aqueous filtration; dmso; 400MHz
45 Completed 200407-jwd 8 N 1H 1H experiment jwd 00:01:00 Supervisor Morris jwd-H109-NH2-pyrazole; column; dmso; 400MHz
46 Completed 200407-sag 1 N 1H 1H experiment sag 00:01:00 Supervisor Kumar GSN-2-51
47 Completed 200407-yim 1 N 1H 1H experiment yim 00:01:00 Supervisor Stenzel z-lysine nca monomer old sample check
48 Completed 200407-dit 1 N 1H 1H experiment dit 00:01:00 Supervisor Kumar DS-1-16
49 Completed 200407-jwd 9 N 1H 1H experiment jwd 00:01:00 Supervisor Morris jwd; napthyl IP; cdcl3; 400MHz
49 Completed 200407-jwd 10 N 13C.night 13C experiment; use td0 to add scans jwd 01:02:11 Supervisor Morris jwd; napthyl IP; cdcl3; 100MHz
50 Completed 200407-jwd 11 N 1H 1H experiment jwd 00:01:00 Supervisor Morris jwd; 7-quin IP; cdcl3; 400MHz
50 Completed 200407-jwd 12 N 13C.night 13C experiment; use td0 to add scans jwd 01:02:11 Supervisor Morris jwd; 7-quin IP; cdcl3; 100MHz
51 Completed 200407-jwd 13 N 1H 1H experiment jwd 00:01:00 Supervisor Morris jwd; 7-isoquin IP; cdcl3; 400MHz
51 Running 200407-jwd 14 N 13C.night 13C experiment; use td0 to add scans jwd 01:02:11 Supervisor Morris jwd; 7-isoquin IP; cdcl3; 100MHz
52 Submitted 200407-jwd 15 N 1H 1H experiment jwd 00:01:00 Supervisor Morris jwd; 5-quin IP; cdcl3; 400MHz
52 Submitted 200407-jwd 16 N 13C.night 13C experiment; use td0 to add scans jwd 01:02:11 Supervisor Morris jwd; 5-quin IP; cdcl3; 100MHz
53 Submitted 200407-jwd 17 N 1H 1H experiment jwd 00:01:00 Supervisor Morris jwd; 5-isoquin IP; cdcl3; 400MHz
53 Submitted 200407-jwd 18 N 13C.night 13C experiment; use td0 to add scans jwd 01:02:11 Supervisor Morris jwd; 5-isoquin IP; cdcl3; 100MHz
54 Submitted 200407-jwd 19 N 13C.night 13C experiment; use td0 to add scans jwd 02:04:18 Supervisor Morris Jwd-H103-Nphenylpyrazole; dmf; 100MHz
55 Submitted 200407-nnt 2 N 1H 1H experiment nnt 00:01:00 Supervisor Nguyen NT030
55 Submitted 200407-nnt 3 N 13C.night 13C experiment; use td0 to add scans nnt 01:02:11 Supervisor Nguyen NT030
55 Submitted 200407-nnt 4 N 11B 11B experiment nnt 00:05:05 Supervisor Nguyen NT030
56 Submitted 200407-nnt 5 N 1H 1H experiment nnt 00:01:00 Supervisor Nguyen MS 1
56 Submitted 200407-nnt 6 N 13C.night 13C experiment; use td0 to add scans nnt 01:02:11 Supervisor Nguyen MS 1
56 Submitted 200407-nnt 7 N 11B 11B experiment nnt 00:05:05 Supervisor Nguyen MS 1
57 Submitted 200407-nnt 8 N 1H 1H experiment nnt 00:01:00 Supervisor Nguyen MS2
57 Submitted 200407-nnt 9 N 13C.night 13C experiment; use td0 to add scans nnt 01:02:11 Supervisor Nguyen MS2
57 Submitted 200407-nnt 10 N 11B 11B experiment nnt 00:05:05 Supervisor Nguyen MS2
58 Submitted 200407-rgd 1 N 1H 1H experiment rgd 00:01:00 Supervisor Beves RGD-002-2 BPinF AB
59 Submitted 200407-dbr 4 N 1H 1H experiment dbr 00:01:00 Supervisor Peeks DBR-1-006 pentane wash
59 Submitted 200407-dbr 5 N 1H.cosy dbr 00:10:09 Supervisor Peeks DBR-1-006 pentane wash
60 Submitted 200407-jpj 1 N 1H 1H experiment jpj 00:01:00 Supervisor Kumar triazole
60 Submitted 200407-jpj 2 N 13C.day 13C experiment; 140 scans, 10 minutes jpj 00:10:26 Supervisor Kumar triazole
History List
Holder Time Name ExpNo Experiment User Load Atma Spin Lock Shim Acq Proc Title Remarks
51 18:12:34 200407-jwd 14 13C.night jwd - + + - - - - Supervisor Morris jwd; 7-isoquin IP; cdcl3; 100MHz
51 18:05:56 200407-jwd 13 1H jwd + + + + + + + Supervisor Morris jwd; 7-isoquin IP; cdcl3; 400MHz
50 17:02:23 200407-jwd 12 13C.night jwd - + + - - + + Supervisor Morris jwd; 7-quin IP; cdcl3; 100MHz
50 16:57:28 200407-jwd 11 1H jwd + + + + x + + Supervisor Morris jwd; 7-quin IP; cdcl3; 400MHz Shim failed
49 15:53:58 200407-jwd 10 13C.night jwd - + + - - + + Supervisor Morris jwd; napthyl IP; cdcl3; 100MHz
49 15:47:30 200407-jwd 9 1H jwd + + + + + + + Supervisor Morris jwd; napthyl IP; cdcl3; 400MHz
48 15:02:24 200407-dit 1 1H dit + + + + + + + Supervisor Kumar DS-1-16
47 14:55:02 200407-yim 1 1H yim + + + + + + + Supervisor Stenzel z-lysine nca monomer old sample check
46 14:25:14 200407-sag 1 1H sag + + + + + + + Supervisor Kumar GSN-2-51
45 14:18:26 200407-jwd 8 1H jwd + + + + + + + Supervisor Morris jwd-H109-NH2-pyrazole; column; dmso; 400MHz
44 14:12:57 200407-jwd 7 1H jwd + + + + x + + Supervisor Morris jwd-H109-NH2-pyrazole; aqueous filtration; dmso; 400MHz Shim failed
6 13:43:59 200407-dme 1 1H dme x - - - - - - Supervisor Stenzel Acid 3 crude 7/04/2020 Sample Changer: Error: SKIP_SAMPLE :: Error: No sample in position 6
43 13:37:04 200407-hgf 1 1H hgf + + + + + + + Supervisor Martina HF1.6 re.cryst.NIPAM CDCl3
42 13:28:49 200407-rra 1 1H rra + + + + + + + Supervisor Stenzel RR34_PHEA-Semicarbazide
41 13:16:30 200407-jwd 6 1H13C.hsqc.aded jwd - + + - - + + Supervisor Morris jwd; H103-pyrazole; dmf; 400MHz; HSQC
41 13:06:12 200407-jwd 5 1H jwd + + + + + + + Supervisor Morris jwd; H103-pyrazole; dmf; 400MHz 2
40 12:59:34 200407-pir 2 1H pir + + + + + + + Supervisor Hunter PR3.32 THF-check
39 12:49:13 200407-ydx 4 1H ydx + + + + + + + Supervisor Stenzel DP-C18
38 12:40:54 200407-ydx 3 1H ydx + + + + x + + Supervisor Stenzel PFP-2 Shim failed
37 12:30:33 200407-ydx 2 1H ydx + + + + + + + Supervisor Stenzel PFP-1
36 12:23:19 200407-ydx 1 1H ydx + + + + + + + Supervisor Stenzel Caro - CH22 free radical polymerisation
35 12:17:51 200407-moa 1 1H moa + + + + x + + Supervisor Hunter MOA1.066 CRude (may have Toluene) in CDCl3 Shim failed
34 12:11:12 200407-mjh 9 1H mjh + + + + + + + Supervisor Chapman MH1.14I pA-MA. DP400. 10x cye3.
33 11:56:01 200407-jwd 4 1H jwd + + + + + + + Supervisor Morris jwd; H103-pyraozle; DMF; 400MHz
32 11:47:50 200407-mjh 8 1H mjh + + + + + + + Supervisor Chapman MH1.14H pA-MA/HEMA. 50% HEMA. DP800. 1/800 Cye3.
31 11:40:00 200407-mjh 7 1H mjh + + + + + + + Supervisor Chapman MH1.14G pA-MA/HEMA. 20% HEMA. DP800. 1/800 Cye3.
30 11:32:12 200407-mjh 6 1H mjh + + + + + + + Supervisor Chapman MH1.14F pA-MA/HEMA. 10% HEMA. DP800. 1/800 Cye3.
29 11:24:57 200407-mjh 5 1H mjh + + + + + + + Supervisor Chapman MH1.14E pA-MA. 0% HEMA. DP800. 1/800 Cye3.
28 11:17:33 200407-mjh 4 1H mjh + + + + + + + Supervisor Chapman MH1.14D pA-MA/HEMA. 50% HEMA. DP400. 1/800 Cye3.
27 11:10:25 200407-mjh 3 1H mjh + + + + + + + Supervisor Chapman MH1.14C pA-MA/HEMA. 20% HEMA. DP400. 1/800 Cye3.
26 11:02:35 200407-mjh 2 1H mjh + + + + + + + Supervisor Chapman MH1.14B pA-MA/HEMA. 10% HEMA. DP400. 1/800 Cye3.
25 10:55:40 200407-mjh 1 1H mjh + + + + + + + Supervisor Chapman MH1.14A pA-MA. 0% HEMA. DP400. 1/800 Cye3.
24 10:41:45 200407-pir 1 1H pir + + + + x + + Supervisor Hunter PR3.30 Deprotection HM Shim failed
23 10:26:45 200407-jwd 3 1H jwd + + + + x + + Supervisor Morris jwd; H103-pyrazole; MeOD; 400MHz Shim failed
23 10:12:40 200407-jwd 2 1H jwd + + + + x + + Supervisor Morris jwd; H103-pyrazole; cdcl3/MeOD; 400MHz Shim failed
22 10:02:10 200407-ywa 1 1H ywa + + + + + + + Supervisor Stenzel column fraction check new point
21 09:48:14 200407-jwd 1 1H jwd + + + + x + + Supervisor Morris jwd; H103-pyrazole; cdcl3; 400MHz Shim failed
20 09:30:02 200407-tat 2 1H tat + + + + + + + Supervisor Nguyen CDCl3_P5-A2_C
19 09:24:41 200407-tat 1 1H tat + + + + x + + Supervisor Nguyen CDCl3_P5-A1_C Shim failed
18 09:05:47 200407-shd 2 13C.day shd - + + - - + + Supervisor Nguyen S001S20C3
18 08:58:02 200407-shd 1 1H shd + + + + + + + Supervisor Nguyen S001S20C3
17 08:14:19 200407-nnt 1 1H nnt + + + + + + + Supervisor Nguyen nt031, Blue LED
16 20:14:25 200406-kll 12 1H kll + + + + + + + Supervisor Boyer x35x
15 20:05:59 200406-kll 11 1H kll + + + + + + + Supervisor Boyer x25x
14 19:57:27 200406-kll 10 1H kll + + + + + + + Supervisor Boyer x15x
13 19:49:00 200406-kll 9 1H kll + + + + + + + Supervisor Boyer 35x
12 19:40:33 200406-kll 8 1H kll + + + + + + + Supervisor Boyer 25x
11 19:32:14 200406-kll 7 1H kll + + + + + + + Supervisor Boyer 15x
10 19:24:28 200406-ryl 3 1H ryl + + + + + + + Supervisor Stenzel YDX CDCl3 Dp C18
9 19:17:30 200406-ryl 2 1H ryl + + + + + + + Supervisor Stenzel CARO CH21 after ftnir
8 19:09:34 200406-ryl 1 1H ryl + + + + + + + Supervisor Stenzel CARO CH19 ManAM
5 19:00:55 200406-nnt 5 11B nnt - + + - - + + Supervisor Nguyen NT029
5 17:57:25 200406-nnt 4 13C.night nnt - + + - - + + Supervisor Nguyen NT029
5 17:51:16 200406-nnt 3 1H nnt + + + + + + + Supervisor Nguyen NT029
4 17:44:23 200406-nnt 2 1H nnt + + + + + + + Supervisor Nguyen MS4. TropPF6
3 17:37:22 200406-tty 1 1H tty + + + + + + + Supervisor Kumar Compound check: Piperidine
2 17:30:25 200406-jwd 1 1H jwd + + + + + + + Supervisor Morris jwd; bromo-imidazo-amide; cdcl3; 400MHz
1 17:23:54 200406-kej 2 1H kej + + + + + + + Supervisor Boyer BP-31-72.5m
60 17:17:11 200406-kej 1 1H kej + + + + + + + Supervisor Boyer BP-31-0m
59 17:12:29 200406-hol 2 1H hol + + + + x + + Supervisor Stride Max ester, filtered through silica again in MeOD Shim failed
57 17:05:47 200406-cke 4 1H cke + + + + + + + Supervisor Kim CKL-1-8-1 vial 5 (tail section)
56 17:00:03 200406-cke 1 1H cke + + + + x + + Supervisor Kim CKL-1-8-1 vial 4 (tail section) Shim failed
55 16:51:52 200406-kll 6 1H kll + + + + + + + Supervisor Boyer t0 x35x
54 16:43:07 200406-kll 5 1H kll + + + + + + + Supervisor Boyer t0 x25x
53 16:34:49 200406-kll 4 1H kll + + + + + + + Supervisor Boyer t0 x15x
52 16:27:10 200406-kll 3 1H kll + + + + + + + Supervisor Boyer t0 35x
51 16:19:04 200406-kll 2 1H kll + + + + + + + Supervisor Boyer t0 25x
50 16:11:19 200406-kll 1 1H kll + + + + + + + Supervisor Boyer t0 15x
49 16:02:56 200406-raj 2 1H raj + + + + + + + Supervisor Kumar RKP-9-28(9)-SPOT2
48 15:56:35 200406-raj 1 1H raj + + + + x + + Supervisor Kumar RKP-9-28(9)-SPOT1 Shim failed
47 15:50:09 200406-nnt 1 1H nnt + + + + + + + Supervisor Nguyen NT029
46 15:43:42 200406-dit 1 1H dit + + + + + + + Supervisor Kumar DS-1-5 cyclisation
45 15:37:02 200406-jpj 3 1H jpj + + + + + + + Supervisor Kumar crystalized 14a
44 15:30:25 200406-jpj 2 1H jpj + + + + + + + Supervisor Kumar fluoronated compund 14a
43 15:13:32 200406-jpj 1 13C.day jpj + + + + + + + Supervisor Kumar triazole
42 15:05:14 200406-shs 2 1H shs + + + + + + + Supervisor Kumar shs-3-86
41 14:57:38 200406-shs 1 1H shs + + + + + + + Supervisor Kumar shs-3-78
40 14:37:06 200406-tat 4 1H tat + + + + + + + Supervisor Nguyen CDCl3_P2-A41-2_PTLC_F4
39 14:15:56 200406-tat 3 1H tat - + + + + + + Supervisor Nguyen CDCl3_P2-A41-2_PTLC_F3
39 11:43:37 200406-tat 3 1H tat + + + + + - - Supervisor Nguyen CDCl3_P2-A41-2_PTLC_F3 Automation was stopped by user
38 11:24:24 200406-tat 2 1H tat + + + + x + + Supervisor Nguyen CDCl3_P2-A41-2_PTLC_F2 Shim failed
37 11:03:18 200406-tat 1 1H tat + + + + + + + Supervisor Nguyen CDCl3_P2-A41-2_PTLC_F1
12 10:46:12 200406-moa 5 1H moa + + + + + + + Supervisor Hunter MOA 1.062(Recrystall, CONC) in DMSO
11 10:39:47 200406-moa 4 1H moa + + + + + + + Supervisor Hunter MOA 1.062(Filtered Crude before Recrystall) in CDCl3
10 10:33:23 200406-moa 3 1H moa + + + + + + + Supervisor Hunter MOA 1.062(Recrystall) in CDCl3
9 10:21:39 200406-moa 2 13C.day moa - + + - - + + Supervisor Hunter MOA 1.062(Recrystall, CONC) in CDCl3
9 10:12:28 200406-moa 1 1H moa + + + + + + + Supervisor Hunter MOA 1.062(Recrystall, CONC) in CDCl3
36 09:58:32 200406-hol 1 1H hol + + + + + + + Supervisor Stride Max ester oil in MeOD
35 09:10:17 200406-lzg 3 1H lzg + + + + + + + Supervisor Stenzel pegmema-3 t=0
34 09:03:49 200406-lzg 2 1H lzg + + + + + + + Supervisor Stenzel pegmema-2 t=0
33 08:55:54 200406-lzg 1 1H lzg + + + + + + + Supervisor Stenzel pemema-1 t=0
8 18:42:26 200405-tat 2 1H tat + + + + + + + Supervisor Nguyen CDCl3_P2-A40-2_crude
7 17:37:30 200405-jwd 6 1H.noesy jwd - + + - - x - Supervisor Morris jwd-H103; Nphenyl pyrazole; DMSO; NOESY; 400MHz Acquisition Failed
7 17:25:16 200405-jwd 5 1H13C.hmbc jwd - + + - - + + Supervisor Morris jwd-H103; Nphenyl pyrazole; DMSO; HMBC; 400MHz
7 17:12:51 200405-jwd 4 1H13C.hsqc.aded jwd - + + - - + + Supervisor Morris jwd-H103; Nphenyl pyrazole; DMSO; HSQC; 400MHz
7 17:05:18 200405-jwd 3 1H jwd + + + + + + + Supervisor Morris jwd-H103; Nphenyl pyrazole; DMSO; 400MHz
8 16:20:40 200405-tat 1 1H tat + + + + x + + Supervisor Nguyen TAT_P2-A43_crude Shim failed
7 13:31:53 200405-jwd 2 13C.night jwd + + + + + + + Supervisor Morris jwd-H111-pyrazole; dmso; 100MHz
6 13:10:01 200405-jwd 1 1H jwd + + + + + + + Supervisor Morris jwd; H111-pyrazole; dmso; 400MHz
5 10:32:48 200405-yhv 2 1H yhv + + + + + + + Supervisor Stenzel IS-2
4 10:24:33 200405-yhv 1 1H yhv + + + + + + + Supervisor Stenzel IS-1
3 15:53:26 200404-vgo 1 1H vgo + + + + + + + Supervisor Beves VG-25
2 10:49:33 200404-pan 2 1H pan + + + + + + + Supervisor Gooding 3 arm PEG RAFT agent 27/3/20 batch
1 10:38:07 200404-pan 1 1H pan + + + + + + + Supervisor Gooding 3 arn PEG RAFT agent 23/3/20 batch